Asymmetric Catalysis from a Chinese Perspective by Qi-Lin Zhou, Jian-Hua Xie (auth.), Shengming Ma (eds.)

By Qi-Lin Zhou, Jian-Hua Xie (auth.), Shengming Ma (eds.)

Qi-Lin Zhou and Jian-Hua Xie: Chiral Spiro Catalysts.- Fuk Loi Lam, Fuk Yee Kwong and Albert S. C. Chan: Chiral Phosphorus Ligands with fascinating houses and useful Applications.- Jiang Pan, Hui-Lei Yu, Jian-He Xu, Guo-Qiang Lin: Advances in Biocatalysis: Enzymatic Reactions and Their Applications.- Mei-Xiang Wang: Enantioselective Biotransformations of Nitriles.- guy family Wong, Yiu Chung Yip and Dan Yang: uneven Epoxidation Catalyzed through Chiral Ketones.- W. J. Liu, N. Li and L. Z. Gong: uneven Organocatalysis.- Qing-Hua Fan and Kuiling Ding: Enantioselective Catalysis with Structurally Tunable Immobilized Catalysts.- Chang-Hua Ding, Xue-Long Hou: Transition Metal-Catalyzed uneven Allylation.- Jian Zhou and Yong Tang: Enantioselective Reactions with Trisoxazolines.- Xiang-Ping Hu, Duo-Sheng Wang, Chang-Bin Yu, Yong-Gui Zhou, and Zhuo Zheng: event in uneven Hydrogenation: Synthesis of Chiral Phosphorus Ligands and uneven Hydrogenation of Heteroaromtics.

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Hatzemann A, Fruchtmann R, Mohrs KH, Raddatz S, Müller-Peddinghuas R (1993) Biochem Pharmacol 45:101–111 70. Alexakis A, Bäckvall JE, Krause N, Pàmies O, Diéguez M (2008) Chem Rev 108:2796–2823 71. Jerphagnon T, Pizzuti MG, Minnaard AJ, Feringa BL (2009) Chem Soc Rev 38:1039–1075 72. Bolm C, Hildebrand JP, Muñiz K, Hermanns N (2001) Angew Chem Int Ed 40:3284–3308 73. Bolshan Y, Chen C-Y, Chilenski JR, Gosselin F, Mathre DJ, O’Shea PD, Roy A, Tillyer RD (2004) Org Lett 6:111–114 74. Sakai M, Ueda M, Miyaura N (1998) Angew Chem Int Ed 37:3279–3281 75.

Hou G-H, Xie J-H, Wang L-X, Zhou Q-L (2006) J Am Chem Soc 128:11774–11775 23. Shi W-J, Wang L-X, Fu Y, Zhu S-F, Zhou Q-L (2003) Tetrahedron: Asymmetry 14:3867–3872 24. Duan H-F, Xie J-H, Shi W-J, Zhang Q, Zhou Q-L (2006) Org Lett 8:1479–1481 25. Zhu S-F, Yang Y, Wang L-X, Liu B, Zhou Q-L (2005) Org Lett 7:2333–2335 26. Zhang W, Zhu S-F, Qiao X-C, Zhou Q-L (2008) Chem Asian J 3:2105–2111 27. Xie J-H, Wang L-X, Fu Y, Zhu S-F, Fan B-M, Duan H-F, Zhou Q-L (2003) J Am Chem Soc 125:4404–4405 28. Xie J-H, Duan H-F, Fan B-M, Cheng X, Wang L-X, Zhou Q-L (2006) Adv Synth Catal 346:625–632 29.

7% enantiopurities. Yet, hydrogenation of the (Z)-isomers using the Ru-Xyl-P-Phos catalyst in methanol produced the markedly inferior enantioselectivity under otherwise identical conditions to that of the (E)-isomers. The hydrogenation of (Z)-b-dehydroamino acids using [{(R)-Xyl-P-Phos}RuCl (h6-benzene)]Cl as catalyst was not effective at all in aprotic solvents such as THF and CH2Cl2, and quantitative conversion was observed in MeOH with low ee. In contrast, the Rh catalyst exhibited much higher catalytic activities in THF, converting (Z)-b-alkyl-b-(acylamino)acrylates to the corresponding b-amino acid derivatives under 8 atm of hydrogen pressures and at ambient temperature.

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